Technology Process of Divinylmercury
There total 8 articles about Divinylmercury which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ethynyl halide; Mg;
In
tetrahydrofuran;
N2-atmosphere; slow addn. of alkenyl halide to Mg, stirring and refluxing for 1 h, cooling in ice, addn. of 0.5 equiv. HgCl2, refluxing for 30 min; cooling, addn. of satd. aq. NH4Cl and Et2O, extn. of aq. layer (Et2O), drying combined org. layers (MgSO4), evapn. (vac.), distn. (vac.);
- Guidance literature:
-
With
mercury dichloride;
In
tetrahydrofuran;
2:1 excess of CH2CHMgBr;;