disalicyloyl-disulfane

Base Information

• Chemical Name: disalicyloyl-disulfane
• CAS No.: 860001-20-3
• Molecular Formula: C₁₄H₁₀O₄S₂
• Molecular Weight: 306.363
• Mol file: 860001-20-3.mol

Synonyms:

Chemical Property of disalicyloyl-disulfane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of disalicyloyl-disulfane

There total 4 articles about disalicyloyl-disulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-acetylsalicyloyl chloride (5538-51-2) → disalicyloyl-disulfane (860001-20-3)

Guidance literature:

With sodium hydrogensulfide; ethanol; Behandeln der Reaktionsloesung mit Jod;

DOI:10.1021/ja01258a506

Reference yield:

aspirin (50-78-2,98201-60-6) → disalicyloyl-disulfane (860001-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; thionyl chloride

2: ethanol; sodium hydrogensulfide / Behandeln der Reaktionsloesung mit Jod

With pyridine; sodium hydrogensulfide; thionyl chloride; ethanol;

DOI:10.1021/ja01258a506

Reference yield:

thiosalicyclic acid (7283-41-2) → disalicyloyl-disulfane (860001-20-3)

Guidance literature:

With iron(III) chloride;

upstream raw materials:

thiosalicyclic acid

O-acetylsalicyloyl chloride

aspirin

salicyloyl chloride