(diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I)

Base Information

• Chemical Name: (diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I)
• CAS No.: 114631-71-9
• Molecular Formula: C₄₆H₄₀O₄P₃Rh
• Molecular Weight: 852.648
• Mol file: 114631-71-9.mol

Synonyms:

Chemical Property of (diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I)

There total 1 articles about (diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Wilkinson's catalyst (14694-95-2) + diphenylphosphinoacetic acid (3064-56-0) → (diphenylphosphinoacetato)(diphenylphosphinoacetic acid)triphenylphosphinerhodium(I) (114631-71-9)

Guidance literature:

In benzene; under N2, molar educt ratio 1:2, refluxed for 2 h; concd. to a small vol., addn. of diethyl ether, pptn. filtered off, washed with ether, recrystn. (CHCl3/n-hexane), dried in vac.; elem. anal.;

DOI:10.1016/S0020-1693(00)83686-5

upstream raw materials:

Wilkinson's catalyst

diphenylphosphinoacetic acid