Dodecanamide, N-(2-ethoxy-6-methylphenyl)-2,2-dimethyl-

Base Information

• Chemical Name: Dodecanamide, N-(2-ethoxy-6-methylphenyl)-2,2-dimethyl-
• CAS No.: 114289-42-8
• Molecular Formula: C₂₃H₃₉NO₂
• Molecular Weight: 361.568
• Mol file: 114289-42-8.mol

Synonyms:

Chemical Property of Dodecanamide, N-(2-ethoxy-6-methylphenyl)-2,2-dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dodecanamide, N-(2-ethoxy-6-methylphenyl)-2,2-dimethyl-

There total 2 articles about Dodecanamide, N-(2-ethoxy-6-methylphenyl)-2,2-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo dodecane (112-29-8) → N-(2-Ethoxy-6-methylphenyl)-2,2-dimethyl-dodecanamide (114289-42-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) NaH, diisopropylamine, 2.) n-BuLi, 3.)

2: 89 percent / SOCl₂ / Ambient temperature

3: triethylamine / tetrahydrofuran / Ambient temperature

With n-butyllithium; thionyl chloride; sodium hydride; triethylamine; diisopropylamine; In tetrahydrofuran;

DOI:10.1021/jm00087a016

Reference yield:

2,2-Dimethyl dodecanoic acid (2874-73-9) → N-(2-Ethoxy-6-methylphenyl)-2,2-dimethyl-dodecanamide (114289-42-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / SOCl₂ / Ambient temperature

2: triethylamine / tetrahydrofuran / Ambient temperature

With thionyl chloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/jm00087a016

upstream raw materials:

1-bromo dodecane

2,2-Dimethyl dodecanoic acid

Refernces