benzyl-(3,7-dimethyl-oct-6-enylidene)-amine

Base Information

• Chemical Name: benzyl-(3,7-dimethyl-oct-6-enylidene)-amine
• CAS No.: 42822-89-9
• Molecular Formula: C₁₇H₂₅N
• Molecular Weight: 243.392
• Mol file: 42822-89-9.mol

Synonyms:

Chemical Property of benzyl-(3,7-dimethyl-oct-6-enylidene)-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl-(3,7-dimethyl-oct-6-enylidene)-amine

There total 4 articles about benzyl-(3,7-dimethyl-oct-6-enylidene)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,7-dimethyl-oct-6-enal (106-23-0,26489-02-1) + benzylamine (100-46-9) → benzyl-(3,7-dimethyl-oct-6-enylidene)-amine (42822-89-9) + N-benzyl-3,7-dimethyloct-6-en-1-amine (214211-52-6)

Guidance literature:

With D-Glucose; reductive aminase from Aspergillus oryzae; CDX-901 GDH; NADP; In aq. phosphate buffer; dimethyl sulfoxide; at 30 ℃; for 24h; pH=7; Enzymatic reaction;

DOI:10.1021/jacs.8b11561

Reference yield:

Citronellol (106-22-9) → benzyl-(3,7-dimethyl-oct-6-enylidene)-amine (42822-89-9) + N-benzyl-3,7-dimethyloct-6-en-1-amine (214211-52-6)

Guidance literature:

Multi-step reaction with 2 steps

1: choline oxidase variant AcCO₆; reductive aminase from Aspergillus oryzae; D-Glucose; NADP; CDX-901 GDH / aq. phosphate buffer; dimethyl sulfoxide / 24 h / 30 °C / pH 7 / Enzymatic reaction

2: reductive aminase from Aspergillus oryzae; D-Glucose; NADP; CDX-901 GDH / aq. phosphate buffer; dimethyl sulfoxide / 24 h / 30 °C / pH 7 / Enzymatic reaction

With D-Glucose; reductive aminase from Aspergillus oryzae; CDX-901 GDH; choline oxidase variant AcCO₆; NADP; In aq. phosphate buffer; dimethyl sulfoxide;

DOI:10.1021/jacs.8b11561

Reference yield:

3,7-dimethyl-oct-6-enal (106-23-0,26489-02-1) + benzylamine (100-46-9) → benzyl-(3,7-dimethyl-oct-6-enylidene)-amine (42822-89-9)

Guidance literature:

In benzene; for 8h; Heating;

DOI:10.1016/S0960-894X(01)00396-1

upstream raw materials:

3,7-dimethyl-oct-6-enal

N-butylamine

benzylamine

Citronellol

Downstream raw materials:

N-benzyl-3,7-dimethyloct-6-en-1-amine

Refernces

• 1、 Sundar,Jacob,Bhat, Sujata V,Valecha, Neena,Biswas, Sukla. "Antimalarial t-butylperoxyamines". . p. 2269 - 2272. Retrieved 2007/10/03.