Technology Process of cinnamyldimethyl-<(2Z)-3-methylpenta-2,4-dienyl>ammonium bromide
There total 4 articles about cinnamyldimethyl-<(2Z)-3-methylpenta-2,4-dienyl>ammonium bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetonitrile / 2 h / 0 °C
2: sodium methoxide / dimethylsulfoxide / 1 h / Ambient temperature
3: 12 g / acetonitrile / 0.5 h / Ambient temperature
With
sodium methylate;
In
dimethyl sulfoxide; acetonitrile;
DOI:10.1039/P19800002033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium methoxide / dimethylsulfoxide / 1 h / Ambient temperature
2: 12 g / acetonitrile / 0.5 h / Ambient temperature
With
sodium methylate;
In
dimethyl sulfoxide; acetonitrile;
DOI:10.1039/P19800002033
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium borohydride / aq. NaOH / 2 h / 50 - 60 °C
2: acetonitrile / 2 h / 0 °C
3: sodium methoxide / dimethylsulfoxide / 1 h / Ambient temperature
4: 12 g / acetonitrile / 0.5 h / Ambient temperature
With
sodium tetrahydroborate; sodium methylate;
In
sodium hydroxide; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/P19800002033
