2-Bromo-1,1-diethoxy-3-methylbutane

Base Information

• Chemical Name: 2-Bromo-1,1-diethoxy-3-methylbutane
• CAS No.: 7463-52-7
• Molecular Formula: C9H19 Br O2
• Molecular Weight: 239.153
• NSC Number: 404386
• DSSTox Substance ID: DTXSID10323595
• Mol file: 7463-52-7.mol

Synonyms:2-bromo-1,1-diethoxy-3-methylbutane;7463-52-7;NSC 404386;NSC404386;DTXSID10323595;NSC-404386

Chemical Property of 2-Bromo-1,1-diethoxy-3-methylbutane

Chemical Property:

• Vapor Pressure: 0.0501mmHg at 25°C
• Boiling Point: 243.4°C at 760 mmHg
• Flash Point: 82.3°C
• Density: 1.171g/cm³
• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 238.05684
• Heavy Atom Count: 12
• Complexity: 101

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(C(C(C)C)Br)OCC

Technology Process of 2-Bromo-1,1-diethoxy-3-methylbutane

There total 8 articles about 2-Bromo-1,1-diethoxy-3-methylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovaleraldehyde diethyl acetal (3842-03-3) → 2-bromo-1,1-diethoxy-3-methyl-butane (7463-52-7)

Guidance literature:

With calcium carbonate; at 10 ℃; beim Bromieren;

Reference yield:

orthoformic acid triethyl ester (122-51-0) → 2-bromo-1,1-diethoxy-3-methyl-butane (7463-52-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: CaCO₃ / 10 °C / beim Bromieren

With diethyl ether; calcium carbonate;

Reference yield:

isovaleraldehyde (590-86-3) → 2-bromo-1,1-diethoxy-3-methyl-butane (7463-52-7)

Guidance literature:

With chloroform; bromine; at -25 ℃; und nachfolgender Einw_.von Aethanol in Gegenwart von CaCl₂;

DOI:10.1177/00912700022009657

upstream raw materials:

isovaleraldehyde diethyl acetal

1-ethoxy-2-bromo-1-chloro-3-methyl-butane

sodium ethanolate

isovaleraldehyde

Downstream raw materials:

1,1-diethoxy-3-methyl-2-butene

hydrogen bromide