Technology Process of Hederagonic acid
There total 7 articles about Hederagonic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 50 °C
2: dmap / dichloromethane / 20 °C
3: pyridinium chlorochromate / dichloromethane / 20 °C
4: hydrogenchloride / methanol; acetone / 10 h / 20 °C
5: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C
With
hydrogenchloride; dmap; palladium 10% on activated carbon; hydrogen; potassium carbonate; pyridinium chlorochromate;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2020.113107
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap / dichloromethane / 20 °C
2: pyridinium chlorochromate / dichloromethane / 20 °C
3: hydrogenchloride / methanol; acetone / 10 h / 20 °C
4: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C
With
hydrogenchloride; dmap; palladium 10% on activated carbon; hydrogen; pyridinium chlorochromate;
In
methanol; dichloromethane; acetone;
DOI:10.1016/j.ejmech.2020.113107
