Technology Process of cis-3-bromoflavan
There total 7 articles about cis-3-bromoflavan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 63 mg / tri-n-butyltin hydride / benzene / 0.5 h / Heating; further reagents
2: 0.76 g / aluminium chloride, lithium aluminium hydride / tetrahydrofuran; diethyl ether / 0.33 h / 0 °C
3: 334 mg / N-bromosuccinimide / diethyl ether / 0.75 h
4: 25 mg / aluminium chloride, lithium aluminium hydride / diethyl ether / 12 h / 0 °C
With
N-Bromosuccinimide; lithium aluminium tetrahydride; aluminium trichloride; tri-n-butyl-tin hydride;
In
tetrahydrofuran; diethyl ether; benzene;
- Guidance literature:
-
With
lithium aluminium tetrahydride; aluminium trichloride;
In
diethyl ether;
at 0 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 40 mg / tri-n-butyltin hydride / benzene / 4 h / Heating
2: 0.76 g / aluminium chloride, lithium aluminium hydride / tetrahydrofuran; diethyl ether / 0.33 h / 0 °C
3: 334 mg / N-bromosuccinimide / diethyl ether / 0.75 h
4: 25 mg / aluminium chloride, lithium aluminium hydride / diethyl ether / 12 h / 0 °C
With
N-Bromosuccinimide; lithium aluminium tetrahydride; aluminium trichloride; tri-n-butyl-tin hydride;
In
tetrahydrofuran; diethyl ether; benzene;
