NP(C₆H₅)2NP(C₆H₅)2NWBr₃

Base Information

• Chemical Name: NP(C₆H₅)2NP(C₆H₅)2NWBr₃
• CAS No.: 110589-09-8
• Molecular Formula: C₂₄H₂₀Br₃N₃P₂W
• Molecular Weight: 835.952
• Mol file: 110589-09-8.mol

Synonyms:

Chemical Property of NP(C₆H₅)2NP(C₆H₅)2NWBr₃

Chemical Property:

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Technology Process of NP(C₆H₅)2NP(C₆H₅)2NWBr₃

There total 1 articles about NP(C₆H₅)2NP(C₆H₅)2NWBr₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

tungsten(IV) bromide (14055-81-3) + 1-amido-1,1,3,3-tetraphenyl-4,4-dihydroketadiphosphonitrilium chloride (2960-45-4) → NP(C6H5)2NP(C6H5)2NWBr3 (110589-09-8)

Guidance literature:

In further solvent(s); byproducts: HBr, HCl; addn. of phosphazene salt to WBr4 suspension (liq. bromine); refluxing, 24h; distn.; drying residue in vac.; recrystn. (twice from dry acetonitrile); elem. anal.;

upstream raw materials:

tungsten(IV) bromide

1-amido-1,1,3,3-tetraphenyl-4,4-dihydroketadiphosphonitrilium chloride

Refernces