Ni(C₁₀H₁₃N₃O)2Cl₂

Base Information

• Chemical Name: Ni(C₁₀H₁₃N₃O)2Cl₂
• CAS No.: 104370-37-8
• Molecular Formula: C₂₀H₂₆Cl₂N₆NiO₂
• Molecular Weight: 512.061
• Mol file: 104370-37-8.mol

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Chemical Property of Ni(C₁₀H₁₃N₃O)2Cl₂

Chemical Property:

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Technology Process of Ni(C₁₀H₁₃N₃O)2Cl₂

There total 1 articles about Ni(C₁₀H₁₃N₃O)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

nickel(II) dichloride hydrate + 1-phenyl-propan-2-one semicarbazone (831-84-5) → Ni(C10H13N3O)2Cl2 (104370-37-8)

Guidance literature:

In ethanol; water; mixing of hot aq. ethanolic soln. of nickel(II) salt and the ketone-compd. in 1:2 molar ratio, refluxing for about half an hour; pptn. by cooling, filtn. of ppt., washing (ethanol), drying (electric oven at 60°C); elem. anal.;

upstream raw materials:

1-phenyl-propan-2-one semicarbazone