1,10-Diazachrysene

Base Information

• Chemical Name: 1,10-Diazachrysene
• CAS No.: 218-21-3
• Molecular Formula: C₁₆H₁₀N₂
• Molecular Weight: 230.269
• DSSTox Substance ID: DTXSID50944405
• Nikkaji Number: J1.409.989A
• Wikidata: Q82921624
• Mol file: 218-21-3.mol

Synonyms:1,10-diazachrysene

Chemical Property of 1,10-Diazachrysene

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 230.084398327
• Heavy Atom Count: 18
• Complexity: 304

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC2=C(C3=C(C=C2)C4=C(C=C3)N=CC=C4)N=C1

Technology Process of 1,10-Diazachrysene

There total 5 articles about 1,10-Diazachrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 1,10-Diazachrysene (218-21-3)

Guidance literature:

With sulfuric acid; nitrobenzene; at 155 - 165 ℃;

Reference yield:

1,6-Naphthylenediamine (2243-63-2) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 1,10-Diazachrysene (218-21-3)

Guidance literature:

With sulfuric acid; nitrobenzene; at 155 - 165 ℃;

Reference yield:

7-nitrobenzoquinoline (186268-25-7) → 1,10-Diazachrysene (218-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium/charcoal; aq.-ethanolic HCl / Hydrogenation

2: aqueous H₃aso4; concentrated H₂SO₄

With hydrogenchloride; palladium on activated charcoal; sulfuric acid; orthoarsenic acid;

upstream raw materials:

7-aminobenzoquinoline

glycerol

1,6-Naphthylenediamine

7-nitrobenzoquinoline

Refernces