Technology Process of 1-<1-(phenylsulfonyl)-3-pyrrolyl>-1,2-ethanediol
There total 2 articles about 1-<1-(phenylsulfonyl)-3-pyrrolyl>-1,2-ethanediol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
ethanol;
for 1h;
Yield given;
Ambient temperature;
DOI:10.1248/cpb.40.2338
- Guidance literature:
-
Multi-step reaction with 2 steps
1: SeO2 / dioxane; H2O / 4 h / Heating
2: NaBH4 / ethanol / 1 h / Ambient temperature
With
sodium tetrahydroborate; selenium(IV) oxide;
In
1,4-dioxane; ethanol; water;
DOI:10.1248/cpb.40.2338
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. NaIO4 / diethyl ether / 0.67 h / Ambient temperature
2: 98 percent / tetrahydrofuran / 0.17 h / -20 °C
3: 82 percent / MnO2 / benzene / 1 h / Heating
4: tetrahydrofuran / 1.5 h / -80 - -40 °C
5: 6percent H2SO4 / 0.5 h / Heating
With
manganese(IV) oxide; sodium periodate; sulfuric acid;
In
tetrahydrofuran; diethyl ether; benzene;
DOI:10.1248/cpb.40.2338
