C₆₉H₁₁₅N₁₁O₁₃

Base Information

• Chemical Name: C₆₉H₁₁₅N₁₁O₁₃
• CAS No.: 121584-08-5
• Molecular Formula: C₆₉H₁₁₅N₁₁O₁₃
• Molecular Weight: 1306.74
• Mol file: 121584-08-5.mol

Synonyms:

Chemical Property of C₆₉H₁₁₅N₁₁O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₉H₁₁₅N₁₁O₁₃

There total 3 articles about C₆₉H₁₁₅N₁₁O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclosporine A (59865-13-3,83602-39-5,122090-69-1,126374-36-5) → C69H115N11O13 (121584-08-5,121652-56-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / DMAP / pyridine / 24 °C

2: 90 percent / sodium metaperiodate / OsO₄ / H₂O; dioxane

3: tetrahydrofuran / 2 h / 0 °C

With dmap; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; 1,4-dioxane; pyridine; water;

DOI:10.1016/S0040-4039(01)80693-6

Reference yield:

C64H113N11O13 (83563-94-4,83602-41-9,121652-55-9) → C69H115N11O13 (121584-08-5,121652-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / sodium metaperiodate / OsO₄ / H₂O; dioxane

2: tetrahydrofuran / 2 h / 0 °C

With sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; 1,4-dioxane; water;

DOI:10.1016/S0040-4039(01)80693-6

Reference yield:

C62H109N11O14 (121584-52-9) + triphenyl(phenylmethylene)phosphorane (16721-45-2) → C69H115N11O13 (121584-08-5,121652-56-0)

Guidance literature:

In tetrahydrofuran; at 0 ℃; for 2h;

DOI:10.1016/S0040-4039(01)80693-6

upstream raw materials:

C₆₂H₁₀₉N₁₁O₁₄

triphenyl(phenylmethylene)phosphorane

cyclosporine A

C₆₄H₁₁₃N₁₁O₁₃

Downstream raw materials:

C₆₇H₁₁₃N₁₁O₁₂

C₆₇H₁₁₃N₁₁O₁₂

Refernces