1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride

Base Information

• Chemical Name: 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride
• CAS No.: 71742-12-6
• Molecular Formula: C₂₆H₂₄NO*F
• Molecular Weight: 385.481
• Mol file: 71742-12-6.mol

Synonyms:

Chemical Property of 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride

There total 2 articles about 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,4,6-triphenylpyrylium fluoride (71896-15-6) + propan-1-ol-3-amine (156-87-6) → 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride (71742-12-6)

Guidance literature:

With sodium; In ethanol; benzene; for 12h; Heating;

Reference yield:

1,3,5-triphenylpent-2-ene-1,5-dione (23800-57-9,76162-49-7) → 1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride (71742-12-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / 40percent HF / toluene / 12 h

2: 75 percent / sodium / benzene; ethanol / 12 h / Heating

With hydrogen fluoride; sodium; In ethanol; toluene; benzene;

Reference yield: 37.0%

1-(3-Hydroxy-propyl)-2,4,6-triphenyl-pyridinium; fluoride (71742-12-6) → 3-fluoropropane-1-ol (462-43-1)

Guidance literature:

at 60 ℃; under 760 Torr;

upstream raw materials:

2,4,6-triphenylpyrylium fluoride

propan-1-ol-3-amine

1,3,5-triphenylpent-2-ene-1,5-dione

Downstream raw materials:

3-fluoropropane-1-ol

Refernces