difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate)

Base Information

• Chemical Name: difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate)
• CAS No.: 1080673-10-4
• Molecular Formula: C₄₂H₄₈Cl₂F₂N₄O₆V
• Molecular Weight: 864.711
• Mol file: 1080673-10-4.mol

Synonyms:

Chemical Property of difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate)

There total 1 articles about difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

vanadium(IV) fluoride (10049-16-8) + cetirizine dihydrochloride (83881-52-1,130018-87-0,163837-48-7) → difluorovanadium(IV)(2-[4-[(4-chlorophenyl)phenylmethyl]-1-piperazinyl]ethoxy acetate) (1080673-10-4)

Guidance literature:

In methanol; methanolic soln. of VF4 added to methanolic soln. of C21H25O3N2Cl dropwise with stirring, mixt. had pH 3, refluxed for 2 h, kept overnight with stirring at room temp.; solvent removed on a rotary apparatus under reduced pressure; recrystn. (MeOH/n-hexane, 1/1); elem. anal.;

DOI:10.1134/S1070328407080052

upstream raw materials:

vanadium(IV) fluoride

cetirizine dihydrochloride

Refernces