Technology Process of C51H74N5O11PS
There total 8 articles about C51H74N5O11PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / diethyl ether / 2 h / Cooling with ice
2: sodium azide / ethanol / 10 h / Reflux
3: water; triphenylphosphine / 1,4-dioxane / 10 h / 20 °C
4: sodium hydroxide / 1,4-dioxane / 10 h / 80 °C / Inert atmosphere
5: triethylamine / N,N-dimethyl-formamide / 1 h
6: 1H-tetrazole / acetonitrile / 1 h / Inert atmosphere
With
1H-tetrazole; sodium azide; water; triethylamine; triphenylphosphine; sodium hydroxide;
In
1,4-dioxane; diethyl ether; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/15257770.2011.587702
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / 1,4-dioxane / 1 h / Inert atmosphere; Cooling with ice
2: sodium hydroxide / 1,4-dioxane / 10 h / 80 °C / Inert atmosphere
3: triethylamine / N,N-dimethyl-formamide / 1 h
4: 1H-tetrazole / acetonitrile / 1 h / Inert atmosphere
With
1H-tetrazole; triethylamine; sodium hydroxide;
In
1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/15257770.2011.587702