Technology Process of C37H40O12
There total 5 articles about C37H40O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 3 h / 50 °C
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Large scale
3: potassium hydroxide; copper(l) iodide; 8-quinolinol / dimethyl sulfoxide / 30 h / 100 °C / Inert atmosphere; Large scale
4: thionyl chloride / 3 h / 50 °C
5: N,N-dimethyl-formamide / Heating
With
copper(l) iodide; 8-quinolinol; thionyl chloride; potassium carbonate; potassium hydroxide;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1055/s-0032-1317527
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Large scale
2: potassium hydroxide; copper(l) iodide; 8-quinolinol / dimethyl sulfoxide / 30 h / 100 °C / Inert atmosphere; Large scale
3: thionyl chloride / 3 h / 50 °C
4: N,N-dimethyl-formamide / Heating
With
copper(l) iodide; 8-quinolinol; thionyl chloride; potassium carbonate; potassium hydroxide;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1055/s-0032-1317527
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide; copper(l) iodide; 8-quinolinol / dimethyl sulfoxide / 30 h / 100 °C / Inert atmosphere; Large scale
2: thionyl chloride / 3 h / 50 °C
3: N,N-dimethyl-formamide / Heating
With
copper(l) iodide; 8-quinolinol; thionyl chloride; potassium hydroxide;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1055/s-0032-1317527
