2-epi-valiolone

Base Information

• Chemical Name: 2-epi-valiolone
• CAS No.: 1384518-63-1
• Molecular Formula: C₇H₁₂O₆
• Molecular Weight: 192.169
• Mol file: 1384518-63-1.mol

Synonyms:

Chemical Property of 2-epi-valiolone

Chemical Property:

Purity/Quality:

>95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-epi-valiolone

There total 2 articles about 2-epi-valiolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2L-(2,3/4,5)-2,3,4-tri-O-benzyl-5-C-benzyloxymethyl-2,3,4,5-tetrahydroxycyclohexanone (306968-48-9) → 2-epi-valiolone (1384518-63-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; water; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja3041866

Reference yield:

D-sedoheptulose-7-phosphate (69975-90-2,90196-61-5,2646-35-7) → 2-epi-valiolone (1384518-63-1)

Guidance literature:

With purine nucleoside phosphorilase; NAD; cobalt(II) chloride; at 28 ℃; pH=7.5; Reagent/catalyst; Kinetics; Inert atmosphere; aq. buffer; Enzymatic reaction;

DOI:10.1021/ja3041866

upstream raw materials:

D-sedoheptulose-7-phosphate

2L-(2,3/4,5)-2,3,4-tri-O-benzyl-5-C-benzyloxymethyl-2,3,4,5-tetrahydroxycyclohexanone

Refernces