PtCl₂((C₆H₅)2P)2CHCH₂OCH₂CH₂C₄H₃S

Base Information

• Chemical Name: PtCl₂((C₆H₅)2P)2CHCH₂OCH₂CH₂C₄H₃S
• CAS No.: 146162-15-4
• Molecular Formula: C₃₂H₃₀Cl₂OP₂PtS
• Molecular Weight: 790.589
• Mol file: 146162-15-4.mol

Synonyms:

Chemical Property of PtCl₂((C₆H₅)2P)2CHCH₂OCH₂CH₂C₄H₃S

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of PtCl₂((C₆H₅)2P)2CHCH₂OCH₂CH₂C₄H₃S

There total 1 articles about PtCl₂((C₆H₅)2P)2CHCH₂OCH₂CH₂C₄H₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-(2-hydroxyethyl)thiophene (13781-67-4) + Cl2Pt((PPh2)2C=CH2) (103237-84-9) → PtCl2((C6H5)2P)2CHCH2OCH2CH2C4H3S (146162-15-4)

Guidance literature:

With catalyst: N(CH₂CH₃)3; In dichloromethane; addn. of alcohol (65-fold) and NEt3 to a soln. of metal-complex in CH2Cl2, react. at room temp. for 7 d; monitoring of react. by NMR; reverse react. on heating in vac.; evapn. (reduced pressure), trituration with Et2O, filtration, recrystn. from acetone-Et2O, drying (vac.); elem. anal.; product not pure;

DOI:10.1039/DT9920003403

upstream raw materials:

3-(2-hydroxyethyl)thiophene

Cl₂Pt((PPh₂)2C=CH₂)

Refernces