phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol

Base Information

• Chemical Name: phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol
• CAS No.: 117592-40-2
• Molecular Formula: C₁₅H₂₀O₄
• Molecular Weight: 264.321
• Mol file: 117592-40-2.mol

Synonyms:

Chemical Property of phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol

There total 1 articles about phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolane (5754-34-7) + phenylacetyl chloride (103-80-0) → phenylacetate ester of 3,4-isopropylidenedioxy butan-1-ol (117592-40-2)

Guidance literature:

With pyridine; In dichloromethane; Yield given; 1.) 0 deg C, 15 min, 2.) room temp., overnight;

DOI:10.1016/S0040-4020(01)81708-7

upstream raw materials:

4-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolane

phenylacetyl chloride

Refernces