(+/-)-1-hydroxy-1-phenyl-acetone semicarbazone

Base Information

• Chemical Name: (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone
• CAS No.: 7624-52-4
• Molecular Formula: C₁₀H₁₃N₃O₂
• Molecular Weight: 207.232
• Mol file: 7624-52-4.mol

Synonyms:

Chemical Property of (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone

There total 3 articles about (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(RS)-1-hydroxy-1-phenylpropan-2-one (90-63-1) → (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone (7624-52-4)

Guidance literature:

DOI:10.1021/ja01257a059 DOI:10.1021/ja01340a033 DOI:10.1039/jr9300001232

Reference yield:

semicarbazide hydrochloride (563-41-7) → (R)-1-hydroxy-1-phenyl-acetone semicarbazone (7624-52-4)

Guidance literature:

With water; sodium hydrogencarbonate;

Reference yield:

1-Phenyl-2-propyn-1-ol (4187-87-5) → (+/-)-1-hydroxy-1-phenyl-acetone semicarbazone (7624-52-4)

Guidance literature:

Multi-step reaction with 2 steps

1: HgSO₄; water / zuletzt unter Erwaermen

With water; mercury(II) sulfate;

upstream raw materials:

(RS)-1-hydroxy-1-phenylpropan-2-one

1-Phenyl-2-propyn-1-ol

semicarbazide hydrochloride