tributylgermyl (trifluoroacetoxy)phenylacetate

Base Information

• Chemical Name: tributylgermyl (trifluoroacetoxy)phenylacetate
• CAS No.: 184483-91-8
• Molecular Formula: C₂₂H₃₃F₃GeO₄
• Molecular Weight: 491.087
• Mol file: 184483-91-8.mol

Synonyms:

Chemical Property of tributylgermyl (trifluoroacetoxy)phenylacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tributylgermyl (trifluoroacetoxy)phenylacetate

There total 1 articles about tributylgermyl (trifluoroacetoxy)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

tri-n-butylgermanium bromide (2117-37-5) + (trifluoroacetoxy)phenylacetic acid (95481-30-4) → tributylgermyl (trifluoroacetoxy)phenylacetate (184483-91-8)

Guidance literature:

With triethylamine; In diethyl ether; benzene; byproducts: trimethylammonium bromide; soln. of Ge-compd. and amine heating to boil, addn. of ether soln. of acid (stirring), refluxing (30 min), cooling to room temperature; petroleum ether addn., ammonium bromide sepn., residue distillation; elem. anal.;

upstream raw materials:

tri-n-butylgermanium bromide

(trifluoroacetoxy)phenylacetic acid

Refernces