ethylmethylphenylphosphine-borane

Base Information Edit

Chemical Name:ethylmethylphenylphosphine-borane
CAS No.:882535-77-5
Molecular Formula:C₉H₁₆BP
Molecular Weight:166.011
Hs Code.:
Mol file:882535-77-5.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethylmethylphenylphosphine-borane Edit

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Technology Process of ethylmethylphenylphosphine-borane

There total 5 articles about ethylmethylphenylphosphine-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 74-96-4
ethyl bromide

: 14044-65-6
borane-THF

: 6372-48-1
methylphenylphosphine

: 1148015-48-8,220788-66-9,882535-77-5
ethylmethylphenylphosphine-borane

Guidance literature:: With NaOCH(CH₃)2CH₂CH₂; [RuH(1,2-bis(dimethylphosphino)ethane)((R)-DIFLUORPHOS)][tetraphenylborate]; In tetrahydrofuran; (N2); addn. of phosphine deriv. and benzyl chloride to THF soln. of sodium alcoholate deriv. and ruthenium compd., stirring at room temp. for 1.5-2 h, addn. of THF soln. of borane deriv., stirring at room temp. for 30 min; addn. of water, extn. (ethyl acetate), washing with brine, drying over Na2SO4, filtration, concg., chromy. (silica gel, 70:30 hexanes/ethyl acetate);