2-Benzyliden-6-methylcycloheptanon

Base Information

• Chemical Name: 2-Benzyliden-6-methylcycloheptanon
• CAS No.: 60547-35-5
• Molecular Formula: C₁₅H₁₈O
• Molecular Weight: 214.307
• Mol file: 60547-35-5.mol

Synonyms:

Chemical Property of 2-Benzyliden-6-methylcycloheptanon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Benzyliden-6-methylcycloheptanon

There total 3 articles about 2-Benzyliden-6-methylcycloheptanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 6-oxoheptanoate (30956-41-3) → 2-Benzyliden-6-methylcycloheptanon (60547-35-5)

Guidance literature:

Multi-step reaction with 5 steps

1: NH₄OAc / acetic acid; benzene

2: Al-Hg / diethyl ether

3: NaCN / dimethylsulfoxide

4: K

5: KOH / ethanol

With potassium hydroxide; aluminium amalgam; sodium cyanide; ammonium acetate; potassium; In diethyl ether; ethanol; acetic acid; dimethyl sulfoxide; benzene;

Reference yield:

2-cyano-3-methyl-oct-2-enedioic acid diethyl ester (60547-29-7) → 2-Benzyliden-6-methylcycloheptanon (60547-35-5)

Guidance literature:

Multi-step reaction with 4 steps

1: Al-Hg / diethyl ether

2: NaCN / dimethylsulfoxide

3: K

4: KOH / ethanol

With potassium hydroxide; aluminium amalgam; sodium cyanide; potassium; In diethyl ether; ethanol; dimethyl sulfoxide;

Reference yield:

Ethyl-6-methyl-7-cyanoheptanoat (60547-33-3) → 2-Benzyliden-6-methylcycloheptanon (60547-35-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K

2: KOH / ethanol

With potassium hydroxide; potassium; In ethanol;

upstream raw materials:

ethyl 6-oxoheptanoate

2-cyano-3-methyl-oct-2-enedioic acid diethyl ester

Ethyl-6-methyl-7-cyanoheptanoat

Downstream raw materials:

3-Methyl-2-(4-methyl-pent-3-enyl)-7-[1-phenyl-meth-(E)-ylidene]-cycloheptanone

1-Methyl-2-(4-methyl-pent-3-enyl)-4-[1-phenyl-meth-(E)-ylidene]-cycloheptane