Technology Process of (E)-7-hexadecenyl tosylate
There total 4 articles about (E)-7-hexadecenyl tosylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide
2.1: toluene-4-sulfonic acid / methanol
3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethylene glycol dimethyl ether / 10 - 140 °C / Inert atmosphere
3.2: Cooling with ice
4.1: pyridine / 4 h / 0 - 5 °C
With
pyridine; lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethylene glycol dimethyl ether;
DOI:10.1016/j.tet.2012.03.002
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide
2.1: toluene-4-sulfonic acid / methanol
3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethylene glycol dimethyl ether / 10 - 140 °C / Inert atmosphere
3.2: Cooling with ice
4.1: pyridine / 4 h / 0 - 5 °C
With
pyridine; lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethylene glycol dimethyl ether;
DOI:10.1016/j.tet.2012.03.002
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / methanol
2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethylene glycol dimethyl ether / 10 - 140 °C / Inert atmosphere
2.2: Cooling with ice
3.1: pyridine / 4 h / 0 - 5 °C
With
pyridine; lithium aluminium tetrahydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; diethylene glycol dimethyl ether;
DOI:10.1016/j.tet.2012.03.002
