Technology Process of 3-{[1-(5-Phenyl-isoxazol-3-yl)-meth-(Z)-ylidene]-amino}-propionic acid ethyl ester
There total 4 articles about 3-{[1-(5-Phenyl-isoxazol-3-yl)-meth-(Z)-ylidene]-amino}-propionic acid ethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 57 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
2: triethylamine, MgSO4 / CH2Cl2 / 1.) O deg C, 2.) room temp. 12 h
With
magnesium sulfate; triethylamine; pyridinium chlorochromate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / NaBH4 / ethanol / 1.) 0 deg C, 2.) room temp., 3 h.
2: 57 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
3: triethylamine, MgSO4 / CH2Cl2 / 1.) O deg C, 2.) room temp. 12 h
With
sodium tetrahydroborate; magnesium sulfate; triethylamine; pyridinium chlorochromate;
In
ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / NH2OH*HCl / ethanol / 3 h / Heating
2: 82 percent / NaBH4 / ethanol / 1.) 0 deg C, 2.) room temp., 3 h.
3: 57 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
4: triethylamine, MgSO4 / CH2Cl2 / 1.) O deg C, 2.) room temp. 12 h
With
sodium tetrahydroborate; hydroxylamine hydrochloride; magnesium sulfate; triethylamine; pyridinium chlorochromate;
In
ethanol; dichloromethane;
