1-benzyl-3-heptylpyrrole

Base Information

• Chemical Name: 1-benzyl-3-heptylpyrrole
• CAS No.: 151557-96-9
• Molecular Formula: C₁₈H₂₅N
• Molecular Weight: 255.403
• Mol file: 151557-96-9.mol

Synonyms:

Chemical Property of 1-benzyl-3-heptylpyrrole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-benzyl-3-heptylpyrrole

There total 3 articles about 1-benzyl-3-heptylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1,1-Dimethoxy-undec-3-ene (113345-64-5) → 1-benzyl-3-heptylpyrrole (151557-96-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Br₂ / pentane / 0.25 h / -15 °C

2: formic acid / pentane / 2 h / Ambient temperature

3: pentane / Heating

With formic acid; bromine; In pentane;

Reference yield:

3,4-Dibromo-1,1-dimethoxy-undecane → 1-benzyl-3-heptylpyrrole (151557-96-9)

Guidance literature:

Multi-step reaction with 2 steps

1: formic acid / pentane / 2 h / Ambient temperature

2: pentane / Heating

With formic acid; In pentane;

Reference yield:

3,4-Dibromo-undecanal (151558-01-9) + benzylamine (100-46-9) → 1-benzyl-3-heptylpyrrole (151557-96-9)

Guidance literature:

In pentane; for 3h; Yield given; Heating;

DOI:10.1055/s-1993-25993

upstream raw materials:

3,4-Dibromo-undecanal

benzylamine

(E)-1,1-Dimethoxy-undec-3-ene

Downstream raw materials:

3-heptyl-1H-pyrrole

Refernces

• 1、 Kulinkovich, O. G.,Ali, Azzuz,Sorokin, V. L.. "A NEW APPROACH TO THE PRODUCTION OF 3-ALKYLPYRROLES". . p. 1870 - 1873. Retrieved 2007/10/02.