2,4,6-Trinitroanilinoacetyl chloride

Base Information

• Chemical Name: 2,4,6-Trinitroanilinoacetyl chloride
• CAS No.: 202288-33-3
• Molecular Formula: C₈H₅ClN₄O₇
• Molecular Weight: 304.603
• Mol file: 202288-33-3.mol

Synonyms:

Chemical Property of 2,4,6-Trinitroanilinoacetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-Trinitroanilinoacetyl chloride

There total 2 articles about 2,4,6-Trinitroanilinoacetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

2,4,6-Trinitroanilinoacetic acid (1032-44-6) → 2,4,6-Trinitroanilinoacetyl chloride (202288-33-3)

Guidance literature:

With phosphorus pentachloride; In chloroform; for 3h; Heating;

DOI:10.1080/00304949809355328

Reference yield:

2,4,6-trinitrochlorobenzene (88-88-0) → 2,4,6-Trinitroanilinoacetyl chloride (202288-33-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 58 percent / Na₂CO₃, H₂O / acetone / 1 h / 25 °C

2: 53 percent / PCl₅ / CHCl₃ / 3 h / Heating

With phosphorus pentachloride; water; sodium carbonate; In chloroform; acetone;

DOI:10.1080/00304949809355328

Reference yield: 34.0%

1,4-phenylenediamine (106-50-3) + 2,4,6-Trinitroanilinoacetyl chloride (202288-33-3) → 1,4-Bis-<α-(2,4,6-trinitroanilino)acetamido>benzene

Guidance literature:

In N,N-dimethyl-formamide; at 25 ℃; for 3h;

DOI:10.1080/00304949809355328

upstream raw materials:

2,4,6-Trinitroanilinoacetic acid

2,4,6-trinitrochlorobenzene

Refernces