CH(CH₃)CH(CH₃)CHCH₂OH

Base Information

• Chemical Name: CH(CH₃)CH(CH₃)CHCH₂OH
• CAS No.: 123482-31-5
• Molecular Formula: C₆H₁₂O
• Molecular Weight: 100.161
• Mol file: 123482-31-5.mol

Synonyms:

Chemical Property of CH(CH₃)CH(CH₃)CHCH₂OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of CH(CH₃)CH(CH₃)CHCH₂OH

There total 2 articles about CH(CH₃)CH(CH₃)CHCH₂OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethylsulfide borane complex (13292-87-0) + cis-2,3-dimethylmethylenecyclopropane (4866-55-1) + (-)-trans-2,3-dimethylmethylenecyclopropane (5070-00-8) → CH(CH3)CH(CH3)CHCH2OH (123482-31-5) + 3-methylpent-4-en-2-ol (1569-59-1) + 2-cis-3-trans-Dimethyl-cyclopropyl-methanol (23038-04-2,23038-05-3,24382-75-0,123482-31-5)

Guidance literature:

With dihydrogen peroxide; In tetrahydrofuran; under nitrogen, cooled at 0°C, after stirring for 45 min NaOH (3 M) and 30% H2O2 added, stirred for 1 h, water added, saturated with K2CO3; aq. phase extn. (ether), combined org. phase dried, destn. under vacuum; NMR;

DOI:10.1016/0022-328X(88)80667-3

Reference yield:

dimethylsulfide borane complex (13292-87-0) + cis-2,3-dimethylmethylenecyclopropane (4866-55-1) + (-)-trans-2,3-dimethylmethylenecyclopropane (5070-00-8) → CH(CH3)CH(CH3)CHCH2OH (123482-31-5) + 3-methylpent-4-en-2-ol (1569-59-1) + 2-cis-3-trans-Dimethyl-cyclopropyl-methanol (23038-04-2,23038-05-3,24382-75-0,123482-31-5)

Guidance literature:

With dihydrogen peroxide; In tetrahydrofuran; under nitrogen, cooled at 0°C, after stirring for 45 min NaOH (3 M) and 30% H2O2 added, stirred for 1 h, water added, saturated with K2CO3; aq. phase extn. (ether), combined org. phase dried, destn. under vacuum; NMR;

DOI:10.1016/0022-328X(88)80667-3

upstream raw materials:

dimethylsulfide borane complex

cis-2,3-dimethylmethylenecyclopropane

(-)-trans-2,3-dimethylmethylenecyclopropane

Refernces