Technology Process of C54H51N15
There total 4 articles about C54H51N15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium t-butanolate;
In
1,4-dioxane;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1021/jo5003714
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran / 10 h / 20 °C / Reflux
1.2: 6 h / Reflux
2.1: ammonium hydroxide / water / 24 h / 170 °C / Autoclave
3.1: sodium hydride / tetrahydrofuran / 10 h / 20 °C / Reflux
3.2: 3 h / Reflux
4.1: tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium t-butanolate / 1,4-dioxane / 3 h / Inert atmosphere; Reflux
With
ammonium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium hydride; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo5003714
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / 10 h / 20 °C / Reflux
1.2: 3 h / Reflux
2.1: tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium t-butanolate / 1,4-dioxane / 3 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium hydride; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jo5003714
