Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine

Base Information

• Chemical Name: Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine
• CAS No.: 114979-97-4
• Molecular Formula: C₂₇H₃₆N₂O₃
• Molecular Weight: 436.594
• Mol file: 114979-97-4.mol

Synonyms:

Chemical Property of Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine

There total 4 articles about Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

dibutylamine (111-92-2) + 2-{(E)-2-[4-(3-Chloro-propoxy)-phenyl]-vinyl}-6-methoxy-benzooxazole (124941-85-1) → Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine (114979-97-4)

Guidance literature:

at 150 ℃; for 12h;

DOI:10.1021/jm00117a018

Reference yield:

4-(3-chloropropoxy)benzaldehyde (82625-25-0) → Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine (114979-97-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 50percent aq. sodium hydroxide / dimethylsulfoxide / 24 h / Ambient temperature

2: 8 percent / 12 h / 150 °C

With sodium hydroxide; In dimethyl sulfoxide;

DOI:10.1021/jm00117a018

Reference yield:

6-methoxy-2-methyl-benzoxazole (23999-64-6) → Dibutyl-(3-{4-[(E)-2-(6-methoxy-benzooxazol-2-yl)-vinyl]-phenoxy}-propyl)-amine (114979-97-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 50percent aq. sodium hydroxide / dimethylsulfoxide / 24 h / Ambient temperature

2: 8 percent / 12 h / 150 °C

With sodium hydroxide; In dimethyl sulfoxide;

DOI:10.1021/jm00117a018

upstream raw materials:

dibutylamine

2-{(E)-2-[4-(3-Chloro-propoxy)-phenyl]-vinyl}-6-methoxy-benzooxazole

4-(3-chloropropoxy)benzaldehyde

6-methoxy-2-methyl-benzoxazole

Refernces