Technology Process of C21H23ClN2O3
There total 6 articles about C21H23ClN2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / diethyl ether; water / 4 h / 20 °C
2: sodium tetrahydroborate; cobalt(II) chloride / methanol / 0.33 h / 100 °C / Microwave irradiation
3: sodium hydrogencarbonate / tetrahydrofuran / 20 °C
4: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
With
hydrogenchloride; sodium tetrahydroborate; sodium hydride; sodium hydrogencarbonate; cobalt(II) chloride;
In
tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.02.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; cobalt(II) chloride / methanol / 0.33 h / 100 °C / Microwave irradiation
2: sodium hydrogencarbonate / tetrahydrofuran / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
With
sodium tetrahydroborate; sodium hydride; sodium hydrogencarbonate; cobalt(II) chloride;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.02.009