1-phenylhomogermatrane

Base Information

• Chemical Name: 1-phenylhomogermatrane
• CAS No.: 76705-71-0
• Molecular Formula: C₁₃H₁₉GeNO₃
• Molecular Weight: 309.889
• Mol file: 76705-71-0.mol

Synonyms:

Chemical Property of 1-phenylhomogermatrane

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 1-phenylhomogermatrane

There total 2 articles about 1-phenylhomogermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenylgermasesquioxane + 2,2'-<(3-hydroxypropyl)imino>bisethanol (4767-14-0) → 1-phenylhomogermatrane (76705-71-0)

Guidance literature:

With potassium hydroxide; In xylene; byproducts: H2O; heated until no more water separated; ether added; filtered off; washed (ether);

Reference yield: 76.0%

3-(trimethylsiloxy)-N,N-bis[2-(trimethylsiloxy)ethyl]propylamine (86845-03-6) + trichlorophenylgermane (1074-29-9) → 1-phenylhomogermatrane (76705-71-0)

Guidance literature:

In chloroform; byproducts: (CH3)3SiCl; boiled for 6 h; solvent removed; dissolved in a little xylene; ether added; filtered off; washed (ether); dried in vac.; elem. anal.;

upstream raw materials:

2,2'-<(3-hydroxypropyl)imino>bisethanol

3-(trimethylsiloxy)-N,N-bis[2-(trimethylsiloxy)ethyl]propylamine

trichlorophenylgermane