Technology Process of C15H17NO5
There total 4 articles about C15H17NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/anie.201309847
- Guidance literature:
-
Multi-step reaction with 4 steps
1: silver perchlorate / acetone; water / 1.5 h / 20 °C
2: tert.-butyl lithium / diethyl ether; pentane / 4 h / -78 - 20 °C / Inert atmosphere
3: benzoic acid methyl ester / diethyl ether / 8 h / 20 °C / UV-irradiation
4: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
pyridine; benzoic acid methyl ester; tert.-butyl lithium; silver perchlorate;
In
diethyl ether; dichloromethane; water; acetone; pentane;
DOI:10.1002/anie.201309847
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tert.-butyl lithium / diethyl ether; pentane / 4 h / -78 - 20 °C / Inert atmosphere
2: benzoic acid methyl ester / diethyl ether / 8 h / 20 °C / UV-irradiation
3: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
pyridine; benzoic acid methyl ester; tert.-butyl lithium;
In
diethyl ether; dichloromethane; pentane;
DOI:10.1002/anie.201309847