Technology Process of C29H40N4O12S
There total 4 articles about C29H40N4O12S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H25N3O7S;
With
triethylamine; isobutyl chloroformate;
In
N,N-dimethyl-formamide;
at -15 ℃;
for 0.25h;
(+)-3,4-diacetyloxy-L-phenylalanine methyl ester hydrochloride;
With
triethylamine;
In
N,N-dimethyl-formamide;
at -15 - 5 ℃;
DOI:10.1007/s00726-010-0804-z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 0 - 5 °C
2.1: trifluoroacetic acid / 2 h / 20 °C
3.1: triethylamine; isobutyl chloroformate / N,N-dimethyl-formamide / 0.25 h / -15 °C
3.2: -15 - 5 °C
With
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; isobutyl chloroformate;
In
N,N-dimethyl-formamide;
DOI:10.1007/s00726-010-0804-z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 0 - 5 °C
2.1: trifluoroacetic acid / 2 h / 20 °C
3.1: triethylamine; isobutyl chloroformate / N,N-dimethyl-formamide / 0.25 h / -15 °C
3.2: -15 - 5 °C
With
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; isobutyl chloroformate;
In
N,N-dimethyl-formamide;
DOI:10.1007/s00726-010-0804-z