C₂₃H₃₃NO

Base Information

• Chemical Name: C₂₃H₃₃NO
• CAS No.: 1146191-02-7
• Molecular Formula: C₂₃H₃₃NO
• Molecular Weight: 339.521
• Mol file: 1146191-02-7.mol

Synonyms:

Chemical Property of C₂₃H₃₃NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₃NO

There total 4 articles about C₂₃H₃₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H31NO → C23H33NO (1146191-02-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmcl.2016.03.042

Reference yield:

4-tert-Butylbenzaldehyde (939-97-9) → C23H33NO (1146191-02-7)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / 0 °C

2: tert.-butylhydroperoxide; chromium(III) oxide / dichloromethane / 1 h / 20 °C

3: lithium perchlorate / neat (no solvent) / 1 h / 20 °C

4: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

With tert.-butylhydroperoxide; chromium(III) oxide; sodium tetrahydroborate; lithium perchlorate; In tetrahydrofuran; methanol; dichloromethane; 3: |Michael Addition;

DOI:10.1016/j.bmcl.2016.03.042

Reference yield:

1-(4-(tert-butyl)phenyl)prop-2-en-1-ol (863029-85-0) → C23H33NO (1146191-02-7)

Guidance literature:

Multi-step reaction with 3 steps

1: tert.-butylhydroperoxide; chromium(III) oxide / dichloromethane / 1 h / 20 °C

2: lithium perchlorate / neat (no solvent) / 1 h / 20 °C

3: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

With tert.-butylhydroperoxide; chromium(III) oxide; sodium tetrahydroborate; lithium perchlorate; In methanol; dichloromethane; 2: |Michael Addition;

DOI:10.1016/j.bmcl.2016.03.042

upstream raw materials:

4-tert-Butylbenzaldehyde

1-(4-(tert-butyl)phenyl)prop-2-en-1-ol

1-(4-(tert-butyl)phenyl)prop-2-en-1-one

Refernces