Technology Process of 1-(2,2-diethyl-4-methylcyclobutoxy)-4-(3-(4-(prop-1-en-1-yloxy)-phenyl)propyl)benzene
There total 10 articles about 1-(2,2-diethyl-4-methylcyclobutoxy)-4-(3-(4-(prop-1-en-1-yloxy)-phenyl)propyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
dimethyl sulfoxide;
at 20 ℃;
for 6h;
DOI:10.1021/jo3028246
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dilithium tetrachlorocuprate / tetrahydrofuran / 16 h / 0 - 20 °C
2: boron tribromide / dichloromethane / 16 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 60 °C
4: potassium tert-butylate / dimethyl sulfoxide / 6 h / 20 °C
5: lithium perchlorate / nitromethane / Electrolysis
With
dilithium tetrachlorocuprate; potassium tert-butylate; lithium perchlorate; boron tribromide; potassium carbonate;
In
tetrahydrofuran; nitromethane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
1: |Grignard Reaction;
DOI:10.1021/jo3028246
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron tribromide / dichloromethane / 16 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 60 °C
3: potassium tert-butylate / dimethyl sulfoxide / 6 h / 20 °C
4: lithium perchlorate / nitromethane / Electrolysis
With
potassium tert-butylate; lithium perchlorate; boron tribromide; potassium carbonate;
In
nitromethane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo3028246