tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose

Base Information

• Chemical Name: tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose
• CAS No.: 121292-31-7
• Molecular Formula: C₃₅H₃₆O₁₄S₄
• Molecular Weight: 808.926
• Mol file: 121292-31-7.mol

Synonyms:

Chemical Property of tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose

There total 2 articles about tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl-α-D-manno-[2]heptulopyranoside (108942-61-6) → tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose (121292-31-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous KOH-solution

2: pyridine

With pyridine; potassium hydroxide;

DOI:10.1021/ja01567a062

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + 2,7-anhydro-manno-2-heptulopyranose (7739-21-1,5397-35-3) → tetrakis-O-(toluene-4-sulfonyl)-β-D-manno-2,7-anhydro-[2]heptulopyranose (121292-31-7)

Guidance literature:

With pyridine;

DOI:10.1021/ja01567a062

upstream raw materials:

p-toluenesulfonyl chloride

2,7-anhydro-manno-2-heptulopyranose

phenyl-α-D-manno-[2]heptulopyranoside