o-Methylsulfon-propiophenon

Base Information

• Chemical Name: o-Methylsulfon-propiophenon
• CAS No.: 91061-66-4
• Molecular Formula: C₁₀H₁₂O₃S
• Molecular Weight: 212.269
• Mol file: 91061-66-4.mol

Synonyms:

Chemical Property of o-Methylsulfon-propiophenon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-Methylsulfon-propiophenon

There total 11 articles about o-Methylsulfon-propiophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(methylsulfanyl)benzaldehyde (7022-45-9) → o-Methylsulfon-propiophenon (91061-66-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. H₂O₂, AcOH

2: diethyl ether

With dihydrogen peroxide; acetic acid; In diethyl ether;

Reference yield:

o-Methylsulfon-ω-diazo-acetophenon (90417-64-4) → o-Methylsulfon-propiophenon (91061-66-4)

Guidance literature:

Multi-step reaction with 4 steps

1: KOAc

2: LiAlH₄ / diethyl ether

3: Pb(OAc)4 / benzene

4: diethyl ether

With lead(IV) acetate; lithium aluminium tetrahydride; potassium acetate; In diethyl ether; benzene;

Reference yield:

ω-Acetoxy-o-methylsulfon-acetophenon (111211-66-6) → o-Methylsulfon-propiophenon (91061-66-4)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether

2: Pb(OAc)4 / benzene

3: diethyl ether

With lead(IV) acetate; lithium aluminium tetrahydride; In diethyl ether; benzene;

upstream raw materials:

Diazoethan

2-methylsulphonylbenzaldehyde

2-(methylsulfanyl)benzaldehyde

2-(methylsulfonyl)benzoic acid