10-chloro-neoisopulegol

Base Information

• Chemical Name: 10-chloro-neoisopulegol
• CAS No.: 74514-24-2
• Molecular Formula: C₁₀H₁₇ClO
• Molecular Weight: 188.697
• Mol file: 74514-24-2.mol

Synonyms:

Chemical Property of 10-chloro-neoisopulegol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-chloro-neoisopulegol

There total 8 articles about 10-chloro-neoisopulegol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

isopulegol (89-79-2,7786-67-6,18674-65-2,20549-46-6,21290-09-5,29141-10-4,50373-36-9,59905-53-2,59905-54-3,96612-21-4,104870-56-6,121468-66-4,122517-60-6,122517-61-7,144541-38-8) → 10-chloroisopulegol (74514-24-2,121842-96-4,121842-97-5,139721-76-9)

Guidance literature:

With sulfuryl dichloride; sodium carbonate; In dichloromethane; at 0 ℃; for 0.333333h;

Reference yield: 70.0%

(+)-neoisopulegol (20549-46-6) → 10-chloro-neoisopulegol (74514-24-2,121842-96-4,121842-97-5,139721-76-9)

Guidance literature:

With calcium hypochlorite; carbon dioxide; In dichloromethane;

Reference yield: 67.0%

(+)-isopulegol (104870-56-6) → (1S,2R,5S)-2-(1-Chloromethyl-vinyl)-5-methyl-cyclohexanol (74514-24-2,121842-96-4,121842-97-5,139721-76-9)

Guidance literature:

With hypochloric acid; In dichloromethane;

DOI:10.1016/S0040-4039(00)71427-4

upstream raw materials:

(+)-isopulegol

isopulegol

ethylene glycol

isopulegol

Downstream raw materials:

(+)-menthofuran

10-chloropulegone

10-chloroisopulegone

Refernces

• 1、 Brocksom, Timothy J.,Santos, Reginaldo B. dos,Varanda, Newton A.,Brocksom, Ursula. "AN EFFICIENT SYNTHESIS OF MONOTERPENE α-METHYLENE-γ-BUTYROLACTONES". . p. 1403 - 1410. Retrieved 2007/10/02.
• 2、 Hegde, Shridhar G.,Vogel, Martin K.,Saddler, John,Hrinyo, Tanya,Rockwell, Ned,et al.. "THE REACTION OF HYPOCHLOROUS ACID WITH OLEFINS. A CONVENIENT SYNTHESYS OF ALLYLIC CHLORIDES". . p. 441 - 444. Retrieved 2007/10/02.