Technology Process of C18H24O6S
There total 10 articles about C18H24O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: acetic anhydride / 140 °C
2: 78 percent / NaBH4 / H2O; tetrahydrofuran
3: Jones oxidation
4: 83 percent / acetalization
5: 1.) diisobutylaluminum hydride / 2.) toluene, 100 deg C
6: K2CO3 / methanol / 50 °C
7: LiAlH4 / diethyl ether
8: tosylation
With
sodium tetrahydroborate; lithium aluminium tetrahydride; diisobutylaluminium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; diethyl ether; water; acetic anhydride;
DOI:10.1248/cpb.32.805
- Guidance literature:
-
Multi-step reaction with 8 steps
1: metaphospholic acid / 200 °C
2: 78 percent / NaBH4 / H2O; tetrahydrofuran
3: Jones oxidation
4: 83 percent / acetalization
5: 1.) diisobutylaluminum hydride / 2.) toluene, 100 deg C
6: K2CO3 / methanol / 50 °C
7: LiAlH4 / diethyl ether
8: tosylation
With
sodium tetrahydroborate; lithium aluminium tetrahydride; diisobutylaluminium hydride; potassium carbonate; meta-phosphoric acid;
In
tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1248/cpb.32.805
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Jones oxidation
2: 83 percent / acetalization
3: 1.) diisobutylaluminum hydride / 2.) toluene, 100 deg C
4: K2CO3 / methanol / 50 °C
5: LiAlH4 / diethyl ether
6: tosylation
With
lithium aluminium tetrahydride; diisobutylaluminium hydride; potassium carbonate;
In
methanol; diethyl ether;
DOI:10.1248/cpb.32.805
