15D-15-phenylsparteine

Base Information

• Chemical Name: 15D-15-phenylsparteine
• CAS No.: 80154-10-5
• Molecular Formula: C₂₁H₃₀N₂
• Molecular Weight: 311.475
• Mol file: 80154-10-5.mol

Synonyms:

Chemical Property of 15D-15-phenylsparteine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 15D-15-phenylsparteine

There total 3 articles about 15D-15-phenylsparteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenyl-2,3-dehydrosparteine (15974-69-3,120019-56-9) → 2-deutero-2-phenylsparteine (80154-10-5)

Guidance literature:

With sodium borodeuteride; In methanol; for 0.25h;

Reference yield:

phenyllithium (591-51-5) → 15D-15-phenylsparteine (80154-10-5,123795-74-4,128352-04-5)

Guidance literature:

Multi-step reaction with 2 steps

2: NaBD₄ / methanol

With sodium borodeuteride; In methanol;

Reference yield:

L-(-)-lupanine (486-88-4) → 15D-15-phenylsparteine (80154-10-5,123795-74-4,128352-04-5)

Guidance literature:

Multi-step reaction with 2 steps

2: NaBD₄ / methanol

With sodium borodeuteride; In methanol;

upstream raw materials:

2-phenyl-2,3-dehydrosparteine

phenyllithium

L-(-)-lupanine

Refernces

• 1、 Boczon, Wladyslaw. "FURTHER STUDIES ON STEREOCHEMISTRY OF SPARTEINE, ITS ISOMERS AND DERIVATIVES. PART VII. STEREOCHEMISTRY OF 2-METHYL- AND 2-PHENYLSPARTEINE AND THE SITES OF THEIR PROTONATION". . p. 339 - 351. Retrieved 2007/10/02.