Al(C₆H₅CH₂NCO(CH₂)5CH₃)3

Base Information

• Chemical Name: Al(C₆H₅CH₂NCO(CH₂)5CH₃)3
• CAS No.: 887487-33-4
• Molecular Formula: C₄₂H₆₀AlN₃O₃
• Molecular Weight: 681.938
• Mol file: 887487-33-4.mol

Synonyms:

Chemical Property of Al(C₆H₅CH₂NCO(CH₂)5CH₃)3

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Al(C₆H₅CH₂NCO(CH₂)5CH₃)3

There total 2 articles about Al(C₆H₅CH₂NCO(CH₂)5CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris(dimethylamido)aluminum(III) dimer (32093-39-3) + heptanoic acid benzylamide (55917-07-2) → Al(C6H5CH2NCO(CH2)5CH3)3 (887487-33-4)

Guidance literature:

In ⁽²⁾H₈-toluene; byproducts: dimethylamine; addn. of amide to a soln. of aluminum compd. in toluene-d8; not isolated, detected by NMR;

DOI:10.1021/ja060331x

Reference yield:

2-Ethylhexylamine (104-75-6) + tris(dimethylamido)aluminum(III) dimer (32093-39-3) + heptanoic acid benzylamide (55917-07-2) → Al(C6H5CH2NCO(CH2)5CH3)3 (887487-33-4) + Al(C6H5CH2NCO(CH2)5CH3)2(CH3(CH2)5CONCH2CH(CH2CH3)(CH2)3CH3) (887487-34-5) + Al(C6H5CH2NCO(CH2)5CH3)(CH3(CH2)5CONCH2CH(CH2CH3)(CH2)3CH3)2 (887487-35-6) + Al(CH3(CH2)5CONCH2CH(CH2CH3)(CH2)3CH3)3 (887487-36-7)

Guidance literature:

In ⁽²⁾H₈-toluene; byproducts: benzylamine, N-(2-ethylhexyl)heptanamide; mixing aluminum compd., amine and amide in toluene-d8 at room temp., heating to 90°Caddn. of amide to a soln. of aluminum compd. in toluene-d8; not isolated, detected by NMR; Kinetics;

DOI:10.1021/ja060331x

upstream raw materials:

2-Ethylhexylamine

tris(dimethylamido)aluminum(III) dimer

heptanoic acid benzylamide

Refernces