Technology Process of C17H15ClFIN4O4
There total 9 articles about C17H15ClFIN4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: potassium carbonate / ethanol
2: 1-methyl-pyrrolidin-2-one; diphenylether / 240 °C
3: trichlorophosphate
4: tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / 1,4-dioxane
5: acetic acid; zinc
6: hydrogenchloride; potassium iodide; sodium nitrite
7: ammonium formate; palladium(II) hydroxide / 1,4-dioxane
8: potassium carbonate / N,N-dimethyl-formamide
9: N-chloro-succinimide / N,N-dimethyl-formamide
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); N-chloro-succinimide; ammonium formate; palladium(II) hydroxide; potassium carbonate; acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; sodium t-butanolate; zinc; sodium nitrite; trichlorophosphate;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; diphenylether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.071
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trichlorophosphate
2: tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / 1,4-dioxane
3: acetic acid; zinc
4: hydrogenchloride; potassium iodide; sodium nitrite
5: ammonium formate; palladium(II) hydroxide / 1,4-dioxane
6: potassium carbonate / N,N-dimethyl-formamide
7: N-chloro-succinimide / N,N-dimethyl-formamide
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); N-chloro-succinimide; ammonium formate; palladium(II) hydroxide; potassium carbonate; acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; sodium t-butanolate; zinc; sodium nitrite; trichlorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.071