2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one

Base Information

• Chemical Name: 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one
• CAS No.: 13713-22-9
• Molecular Formula: C₂₉H₄₀O₃
• Molecular Weight: 436.635
• Mol file: 13713-22-9.mol

Synonyms:

Chemical Property of 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one

There total 5 articles about 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

testosterone (58-22-0) → 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one (13713-22-9)

Guidance literature:

Multi-step reaction with 4 steps

1: oxalic acid diethyl ester / durch aufeinanderfolgende Umsetzung mit CH₃I und mit Natriummethylat bzw. Natriumaethylat

2: benzene; toluene-4-sulfonic acid

3: palladium/charcoal; methanol / Hydrogenation_.beim anschliessenden Erwaermen mit wss. HCl

4: pyridine

With pyridine; methanol; palladium on activated charcoal; toluene-4-sulfonic acid; oxalic acid diethyl ester; benzene;

DOI:10.1021/ja01511a040

Reference yield:

17β-hydroxy-2α-methyl-4-androsten-3-one (1452-40-0) → 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one (13713-22-9)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene; toluene-4-sulfonic acid

2: palladium/charcoal; methanol / Hydrogenation_.beim anschliessenden Erwaermen mit wss. HCl

3: pyridine

With pyridine; methanol; palladium on activated charcoal; toluene-4-sulfonic acid; benzene;

DOI:10.1021/ja01511a040

Reference yield:

3,3-ethanediyldioxy-2α-methyl-androst-5-en-17β-ol (19990-45-5) → 2α-methyl-17β-(3-phenyl-propionyloxy)-5α-androstan-3-one (13713-22-9)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium/charcoal; methanol / Hydrogenation_.beim anschliessenden Erwaermen mit wss. HCl

2: pyridine

With pyridine; methanol; palladium on activated charcoal;

DOI:10.1021/ja01511a040

upstream raw materials:

dromostanolone

hydrocinnamic acid chloride

testosterone

17β-hydroxy-2α-methyl-4-androsten-3-one