Technology Process of 3β,5,17β-trihydroxy-5α-androstan-6-one 3β,17β-diacetate
There total 1 articles about 3β,5,17β-trihydroxy-5α-androstan-6-one 3β,17β-diacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrachloromethane; di-tert-butyl chromate; acetic acid;
Reagens 4:Acetanhydrid;
DOI:10.1002/hlca.19520350137
- Guidance literature:
-
With
Perbenzoic acid;
In
chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / SOCl2, pyridine / 0.33 h / 0 °C
2: 82 percent / 10percent KOH/MeOH / methanol / 0.75 h / Ambient temperature
3: NH2OH*HCl, NaOAc / H2O; ethanol / 24 h / Ambient temperature
4: 70 percent / CrO3*pyridine / pyridine / 1 h / Ambient temperature
With
pyridine; methanol; potassium hydroxide; thionyl chloride; chromium trioxide-pyridine complex; hydroxylamine hydrochloride; sodium acetate;
In
pyridine; methanol; ethanol; water;
