Technology Process of 1-(4-chloro-2-nitro-phenyl)-butane-1,3-dione
There total 3 articles about 1-(4-chloro-2-nitro-phenyl)-butane-1,3-dione which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: phosphorus (V)-chloride
2: sodium ethylate; ethanol / <5 / Erhitzen der erhaltenen Natrium-Verbindung des 2-<4-Chlor-2-nitro-benzoyl>-acetessigsaeure-aethylesters mit wss. HCl (4n)
With
ethanol; phosphorus pentachloride; sodium ethanolate;
DOI:10.1021/jo01174a018
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium permanganate; water; pyridine
2: phosphorus (V)-chloride
3: sodium ethylate; ethanol / <5 / Erhitzen der erhaltenen Natrium-Verbindung des 2-<4-Chlor-2-nitro-benzoyl>-acetessigsaeure-aethylesters mit wss. HCl (4n)
With
pyridine; potassium permanganate; ethanol; phosphorus pentachloride; water; sodium ethanolate;
DOI:10.1021/jo01174a018
- Guidance literature:
-
With
ethanol; sodium ethanolate;
Erhitzen der erhaltenen Natrium-Verbindung des 2-<4-Chlor-2-nitro-benzoyl>-acetessigsaeure-aethylesters mit wss. HCl (4n);
DOI:10.1021/jo01174a018