Technology Process of 10-Benzenesulfonyl-7-methyl-1,6-dioxa-spiro[4.5]decane
There total 6 articles about 10-Benzenesulfonyl-7-methyl-1,6-dioxa-spiro[4.5]decane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium dihydrogenphosphate; camphor-10-sulfonic acid;
In
dichloromethane;
for 48h;
Yield given;
Ambient temperature;
DOI:10.1016/0040-4039(88)85307-3
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Mg / tetrahydrofuran
2: Oxone
3: NEt3
4: n-BuLi / tetrahydrofuran / 1 h / -78 °C
5: NaH2PO4, camphorsulphonic acid / CH2Cl2 / 48 h / Ambient temperature
With
Oxone; sodium dihydrogenphosphate; n-butyllithium; camphor-10-sulfonic acid; magnesium; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4039(88)85307-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Oxone
2: NEt3
3: n-BuLi / tetrahydrofuran / 1 h / -78 °C
4: NaH2PO4, camphorsulphonic acid / CH2Cl2 / 48 h / Ambient temperature
With
Oxone; sodium dihydrogenphosphate; n-butyllithium; camphor-10-sulfonic acid; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4039(88)85307-3
