Technology Process of isocorybulbine
There total 5 articles about isocorybulbine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
for 12h;
under 760.051 Torr;
DOI:10.1002/chem.201601245
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / 0.5 h / 20 °C / Inert atmosphere
2: sodium formate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 1 h / 100 °C / Inert atmosphere
3: hydrogen; palladium on activated charcoal / methanol / 12 h / 760.05 Torr
With
tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal; hydrogen; sodium formate; potassium carbonate;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201601245
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium formate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 1 h / 100 °C / Inert atmosphere
2: hydrogen; palladium on activated charcoal / methanol / 12 h / 760.05 Torr
With
tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal; hydrogen; sodium formate;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201601245
